1T4O
Crystal structure of rnt1p dsRBD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-08-02 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 73.815, 68.312, 57.178 |
Unit cell angles | 90.00, 121.91, 90.00 |
Refinement procedure
Resolution | 48.800 - 2.500 |
R-factor | 0.20582 |
Rwork | 0.198 |
R-free | 0.27637 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1t4n |
RMSD bond length | 0.032 |
RMSD bond angle | 2.490 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.800 | 2.560 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 7943 | |
Completeness [%] | 90 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 293 | 0.2M lithium sulfate, 30% PEG 4000, 12% MPD, 0.1M Tris, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K, pH 8.50 |