1T0T
Crystallographic structure of a putative chlorite dismutase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-15 |
Detector | CUSTOM-MADE |
Spacegroup name | I 2 3 |
Unit cell lengths | 202.839, 202.839, 202.839 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.750 |
R-factor | 0.158 |
Rwork | 0.156 |
R-free | 0.19400 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.716 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0001) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.790 |
High resolution limit [Å] | 1.750 | 1.750 |
Number of reflections | 136920 | |
Completeness [%] | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 273 | VAPOR DIFFUSION, HANGING DROP, temperature 273K |