1T00

The structure of thioredoxin from S. coelicolor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-BM
Synchrotron site	APS
Beamline	19-BM
Temperature [K]	100
Detector technology	CCD
Collection date	2004-02-05
Detector	CUSTOM-MADE
Wavelength(s)	0.97918
Spacegroup name	P 21 21 2
Unit cell lengths	43.579, 71.756, 33.187
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.000 - 1.510
R-factor	0.17595
Rwork	0.174
R-free	0.21486
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.014
RMSD bond angle	1.469
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	25.000
High resolution limit [Å]	1.510
Number of reflections	16654

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.6	295	Ammonium acetate, sodium citrate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 295K