1SZI
Crystal Structure of the C-terminus of TIP47
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 95 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 118.746, 118.746, 97.291 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.000 - 2.800 |
| R-factor | 0.238 |
| Rwork | 0.236 |
| R-free | 0.27200 |
| Structure solution method | MIRAS |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.331 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 2.800 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 293.15 | Sodium Citrate, Tris-HCl, sodium Chloride, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K, pH 8.50 |
