1SZH
Crystal Structure of C. elegans HER-1
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2002-09-20 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97931, 0.97917, 0.96866 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.970, 58.930, 99.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.460 - 1.500 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.22700 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.460 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 50045 | |
Completeness [%] | 99.5 | 80.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.3 | 293 | PEG 3350, sodium acetate, ammonijm sulfate, pH 4.3, VAPOR DIFFUSION, HANGING DROP, temperature 293K |