1SYF

ENGINEERING ALTERNATIVE BETA-TURN TYPES IN STAPHYLOCOCCAL NUCLEASE

Experimental procedure

Spacegroup name	P 41
Unit cell lengths	48.500, 48.500, 63.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.800
R-factor	0.168
RMSD bond length	0.015
RMSD bond angle	0.034
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	8.000 *
High resolution limit [Å]	1.800 *
Rmerge	0.072 *
Total number of observations	99105 *
Number of reflections	13515 *
Completeness [%]	100.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	potassium phosphate	10.5 (mM)
2	1	drop	protein	2 (mg/mL)
3	1	drop	pdTp	620 (mM)
4	1	drop		310 (mM)
5	1	reservoir	MPD	25 (%)