1SW5
Crystal structure of ProX from Archeoglobus fulgidus in the ligand free form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-06-11 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9778 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 161.500, 56.500, 116.100 |
Unit cell angles | 90.00, 110.60, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.800 |
R-factor | 0.18785 |
Rwork | 0.186 |
R-free | 0.21439 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1sw1 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.364 |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.25) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 90922 | |
<I/σ(I)> | 10.7 | 3.9 |
Completeness [%] | 99.6 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | magnesium chloride, Tris, PEG 4000, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |