1SW2
Crystal structure of ProX from Archeoglobus fulgidus in complex with glycine betaine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-10-25 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9774 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 75.900, 75.900, 88.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.100 |
| R-factor | 0.20315 |
| Rwork | 0.201 |
| R-free | 0.24870 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1sw1 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.429 |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.25) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.200 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 15622 | |
| <I/σ(I)> | 10.8 | 3.8 |
| Completeness [%] | 99.8 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | PEG 1500, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
