1SUF

Carbon Monoxide Dehydrogenase from Carboxydothermus hydrogenoformans-Inactive state

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron site	MPG/DESY, HAMBURG
Beamline	BW6
Temperature [K]	100
Detector technology	CCD
Collection date	2003-01-01
Detector	MARRESEARCH
Wavelength(s)	1.05
Spacegroup name	C 1 2 1
Unit cell lengths	112.614, 75.004, 71.374
Unit cell angles	90.00, 110.97, 90.00

Refinement procedure

Resolution	8.000 - 1.150
R-factor	0.1521
Rwork	0.152
R-free	0.19020
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	XDS
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.150
Completeness [%]	93.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	298	PEG 3000, 2-Propanol, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K