1SU6
Carbon monoxide dehydrogenase from Carboxydothermus hydrogenoformans: CO reduced state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-01-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 112.154, 75.485, 71.260 |
Unit cell angles | 90.00, 111.20, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.640 |
R-factor | 0.157 |
Rwork | 0.157 |
R-free | 0.20170 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 28.000 |
High resolution limit [Å] | 1.640 |
Number of reflections | 66048 |
Completeness [%] | 95.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 2-Propanol, PEG 3000, Hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |