1SRJ

STRUCTURE-BASED DESIGN OF SYNTHETIC AZOBENZENE LIGANDS FOR STREPTAVIDIN

Experimental procedure

Spacegroup name	I 2 2 2
Unit cell lengths	95.200, 106.500, 47.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.177
RMSD bond length	0.017
RMSD bond angle	0.029
Refinement software	PROFFT

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.079 *
Total number of observations	103092 *
Number of reflections	20894 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		30 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	ammonium sulfate	35-40 (%sat)
2	1	drop	MPD	40 (%(v/v))
3	1	reservoir	MPD	50 (%)