Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-12-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9205, 0.8434, 0.9207 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.500, 53.850, 75.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
Rwork | 0.198 |
R-free | 0.25400 |
Structure solution method | MAD |
RMSD bond length | 0.023 |
RMSD bond angle | 1.350 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 7865 |
Completeness [%] | 97.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | MgCl2, HEPES-Na, PEG 400, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | MgCl2 | ||
2 | 1 | 1 | HEPES-Na | ||
3 | 1 | 1 | PEG 400 | ||
4 | 1 | 2 | MgCl2 | ||
5 | 1 | 2 | PEG 400 |