1SJP
Mycobacterium tuberculosis Chaperonin60.2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-07-15 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9184 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 58.674, 113.825, 79.535 |
| Unit cell angles | 90.00, 94.58, 90.00 |
Refinement procedure
| Resolution | 50.000 - 3.200 |
| R-factor | 0.24359 |
| Rwork | 0.241 |
| R-free | 0.28490 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1KP8.pdb |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.003 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.310 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Rmerge | 0.100 | 0.415 |
| Number of reflections | 17489 | |
| <I/σ(I)> | 20.2 | 2.6 |
| Completeness [%] | 99.5 | 97 |
| Redundancy | 4.99 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
