1SHG
CRYSTAL STRUCTURE OF A SRC-HOMOLOGY 3 (SH3) DOMAIN
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.000, 42.270, 49.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 * - 1.800 |
R-factor | 0.195 |
Rwork | 0.195 |
R-free | 0.27700 |
RMSD bond length | 0.017 |
RMSD bond angle | 2.700 |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 * |
Rmerge | 0.103 * |
Completeness [%] | 96.0 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 3 (mg/ml) | |
2 | 1 | drop | citric acid | 10 (mM) | |
3 | 1 | reservoir | sodium citrate | 90 (mM) | |
4 | 1 | reservoir | bis-Tris propane | 90 (mM) | |
5 | 1 | reservoir | dithiothreitol | 0.9 (mM) | |
6 | 1 | reservoir | EDTA | 0.9 (mM) | |
7 | 1 | reservoir | 0.9 (mM) | ||
8 | 1 | reservoir | ammonium sulfate | 25-30 (%sat) |