1SHD
PEPTIDE INHIBITORS OF SRC SH3-SH2-PHOSPHOPROTEIN INTERACTIONS
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.500, 44.900, 75.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.192 |
Rwork | 0.192 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.800 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.2 * | 22 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | NaOAc | 0.1 (M) | |
2 | 1 | reservoir | PEG4000 | 6-10 (%) | |
3 | 1 | drop | protein | 12-140 (mg/ml) |