1SFG
BINDING OF HEXA-N-ACETYLCHITOHEXAOSE: A POWDER DIFFRACTION STUDY
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X3B1 |
Synchrotron site | NSLS |
Beamline | X3B1 |
Temperature [K] | 296 |
Detector technology | DIFFRACTOMETER |
Collection date | 2001-07-22 |
Detector | CUSTOM-MADE |
Wavelength(s) | 0.700388 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.895, 78.895, 38.254 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - ? |
Data reduction software | PROCESS |
Data scaling software | PROCESS |
Phasing software | GSAS |
Refinement software | GSAS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.130 |
High resolution limit [Å] | 3.220 |
Number of reflections | 2254 |
Completeness [%] | 100.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | rapid precipitation | 6 | 298 | NaCl, Na2HPO4, KH2PO4, hexa-N-acetylchitohexaose, pH 6.0, rapid precipitation, temperature 298K |