1SFB
BINDING OF PENTA-N-ACETYLCHITOPENTAOSE TO HEW LYSOZYME: A POWDER DIFFRACTION STUDY
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X3B1 |
| Synchrotron site | NSLS |
| Beamline | X3B1 |
| Temperature [K] | 296 |
| Detector technology | DIFFRACTOMETER |
| Collection date | 2001-07-21 |
| Detector | CUSTOM-MADE |
| Wavelength(s) | 0.700388 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 79.000, 79.000, 38.137 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - ? |
| Data reduction software | PROCESS |
| Data scaling software | PROCESS |
| Phasing software | GSAS |
| Refinement software | GSAS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.130 |
| High resolution limit [Å] | 3.220 |
| Number of reflections | 2254 |
| Completeness [%] | 100.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | rapid precipitation | 6 | 298 | NaCl, Na2HPO4, KH2PO4, penta-N-acetylchitopentaose, pH 6.0, rapid precipitation, temperature 298K |
