1SF4

BINDING OF N,N'-DIACETYLCHITOBIOSE TO HEW LYSOZYME: A POWDER DIFFRACTION STUDY

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X3B1
Synchrotron site	NSLS
Beamline	X3B1
Temperature [K]	296
Detector technology	DIFFRACTOMETER
Collection date	2001-07-20
Detector	CUSTOM-MADE
Wavelength(s)	0.700388
Spacegroup name	P 43 21 2
Unit cell lengths	78.928, 78.928, 38.178
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - ?
Data reduction software	PROCESS
Data scaling software	PROCESS
Phasing software	GSAS
Refinement software	GSAS

Data quality characteristics

	Overall
Low resolution limit [Å]	40.130
High resolution limit [Å]	2.980
Number of reflections	2797
Completeness [%]	100.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	rapid precipitation	6	298	NaCl, Na2HPO4, KH2PO4, N.N'-diacetylchitobiose, pH 6.0, rapid precipitation, temperature 298K