1SE3
STAPHYLOCOCCAL ENTEROTOXIN B COMPLEXED WITH GM3 TRISACCHARIDE
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 291 |
| Detector technology | AREA DETECTOR |
| Collection date | 1995-02-02 |
| Detector | SIEMENS HI-STAR |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 45.300, 71.000, 78.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.300 |
| R-factor | 0.22 |
| Rwork | 0.220 |
| R-free | 0.33000 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 24.800 * |
| Data reduction software | FBSCALE ((LOCAL VERSION)) |
| Data scaling software | FBSCALE ((LOCAL VERSION)) |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.500 |
| High resolution limit [Å] | 2.250 | 2.250 |
| Number of reflections | 10322 | |
| Completeness [%] | 83.0 | 60 |
| Redundancy | 2.8 | 1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.8 | 24% PEG 4000, 20 MM BORATE BUFFER AT PH 8.8. |
