1SDY

STRUCTURE SOLUTION AND MOLECULAR DYNAMICS REFINEMENT OF THE YEAST CU,ZN ENZYME SUPEROXIDE DISMUTASE

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	105.300, 143.000, 62.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.500
R-factor	0.158
RMSD bond length	0.016
RMSD bond angle	2.912
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	2.500 *
Rmerge	0.060 *
Total number of observations	131852 *
Number of reflections	32538 *
Completeness [%]	98.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mg/ml)
2	1	drop	citrate	0.025 (M)
3	1	drop	PEG4000	6 (%(w/v))
4	1	reservoir	PEG4000	12 (%(w/v))