1SDB
PORCINE DESB1-2 DESPENTAPEPTIDE(B26-B30) INSULIN
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1993-06 |
Detector | SIEMENS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 26.880, 24.500, 28.110 |
Unit cell angles | 90.00, 103.83, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.650 |
R-factor | 0.197 * |
Rwork | 0.203 |
R-free | 0.22030 * |
RMSD bond length | 0.017 |
RMSD bond angle | 0.038 |
Data reduction software | XENGEN |
Refinement software | GPRLSA |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 27.300 |
High resolution limit [Å] | 1.650 |
Rmerge | 0.027 |
Number of reflections | 3829 |
Completeness [%] | 87.1 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 8.4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 5 (mg/ml) | |
2 | 1 | 2 | citrate | 0.05 (M) | |
3 | 1 | 2 | zinc chloride | 0.025 (%) | |
4 | 1 | 2 | acetone | 10 (%) |