1SDB

PORCINE DESB1-2 DESPENTAPEPTIDE(B26-B30) INSULIN

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1993-06
Detector	SIEMENS
Spacegroup name	P 1 21 1
Unit cell lengths	26.880, 24.500, 28.110
Unit cell angles	90.00, 103.83, 90.00

Refinement procedure

Resolution	10.000 - 1.650
R-factor	0.197 *
Rwork	0.203
R-free	0.22030 *
RMSD bond length	0.017
RMSD bond angle	0.038
Data reduction software	XENGEN
Refinement software	GPRLSA

Data quality characteristics

	Overall
Low resolution limit [Å]	27.300
High resolution limit [Å]	1.650
Rmerge	0.027
Number of reflections	3829
Completeness [%]	87.1
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	8.4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	5 (mg/ml)
2	1	2	citrate	0.05 (M)
3	1	2	zinc chloride	0.025 (%)
4	1	2	acetone	10 (%)