1S6Y

2.3A crystal structure of phospho-beta-glucosidase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-BM
Synchrotron site	APS
Beamline	19-BM
Temperature [K]	100
Detector technology	CCD
Collection date	2003-12-10
Detector	SBC-3
Wavelength(s)	0.98080
Spacegroup name	P 2 2 2
Unit cell lengths	61.314, 82.504, 83.504
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.310
R-factor	0.19682
Rwork	0.194
R-free	0.25103
Structure solution method	SAD
RMSD bond length	0.011
RMSD bond angle	1.361
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	REFMAC (5.1.9999)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.380
High resolution limit [Å]	2.300	2.300
Rmerge	0.074	0.343
Number of reflections	18209
Completeness [%]		82.9
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1