1S6M
Conjugative Relaxase Trwc In Complex With Orit DNA. Metal-Bound Structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2003-03-19 |
Detector | MARRESEARCH |
Wavelength(s) | 0.983994 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 92.731, 92.731, 208.855 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.850 - 2.280 |
R-factor | 0.206 |
Rwork | 0.206 |
R-free | 0.24500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1omh |
RMSD bond length | 0.013 |
RMSD bond angle | 1.340 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.264 |
High resolution limit [Å] | 2.280 |
Number of reflections | 24598 |
Completeness [%] | 100.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 296 | 25% PEGMM 2000, 0.2 M AMMONIUM SULPHATE, 0.1 M SODIUM ACETATE, PH 4.6, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 296K |