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1S36

Crystal structure of a Ca2+-discharged photoprotein: Implications for the mechanisms of the calcium trigger and the bioluminescence

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]100
Detector technologyCCD
Collection date2002-11-20
DetectorBRUKER SMART 6000
Wavelength(s)1.5418
Spacegroup nameP 41 21 2
格子定数 [Å]53.445, 53.445, 144.032
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基50.000 - 1.960
R因子0.22459
Rwork0.223
R-free0.25922
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1jf2
結合長の平均二乗偏差(RMSD) [Å]0.012
結合角の平均二乗偏差(RMSD) [度]1.207
Data reduction softwarePROTEUM PLUS
Data scaling softwareLSCALE
Refinement softwareREFMAC (5.1.24)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)72.4602.050
分解能 [Å] (高)1.9601.960
独立反射数15775
<I/σ(I)>9.372.11
完全性 [%]1.00.97
冗長性14.91
結晶化条件
結晶ID方法pH温度溶液条件
1modified microbatch7.52771.5 M tri-sodium citrate, 0.1 M Na-HEPES, pH 7.5, modified microbatch, temperature 277K

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件を2024-09-18に公開中

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