1RY9
Spa15, a Type III Secretion Chaperone from Shigella flexneri
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-06-23 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9196 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.878, 87.682, 58.703 |
Unit cell angles | 90.00, 90.77, 90.00 |
Refinement procedure
Resolution | 43.850 - 1.820 |
R-factor | 0.18272 |
Rwork | 0.181 |
R-free | 0.21108 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.235 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SnB |
Refinement software | REFMAC (5.1.27) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.890 |
High resolution limit [Å] | 1.820 | 1.820 |
Number of reflections | 45246 | |
Completeness [%] | 97.4 | 92.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.3 | 291 | Ammonium Suplhate, ethylene glycol, Guanidium chloride, MES, pH 5.3, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.3 | 291 | Ammonium Suplhate, ethylene glycol, Guanidium chloride, MES, pH 5.3, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.3 | 291 | Ammonium Suplhate, ethylene glycol, Guanidium chloride, MES, pH 5.3, VAPOR DIFFUSION, HANGING DROP, temperature 291K |