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1RY0

Structure of prostaglandin F synthase with prostaglandin D2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-BM
Synchrotron siteAPS
Beamline19-BM
Temperature [K]93
Detector technologyCCD
Collection date2003-08-12
Wavelength(s)1.02
Spacegroup nameP 1
Unit cell lengths46.970, 49.180, 83.520
Unit cell angles73.80, 85.90, 69.80
Refinement procedure
Resolution10.000 - 1.690
R-factor0.208
Rwork0.208
R-free0.24800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3-alpha-HSD (PDB code: 1AFS)
RMSD bond length0.060
RMSD bond angle1.500
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.851)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.750
High resolution limit [Å]1.6901.690
Number of reflections74430
Completeness [%]95.875.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6277PEG 8000, pH 6, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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