1RUE
RHINOVIRUS 14 SITE DIRECTED MUTANT N1219A COMPLEXED WITH ANTIVIRAL COMPOUND WIN 52035
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Detector technology | FILM |
| Collection date | 1991-06 |
| Detector | KODAK |
| Wavelength(s) | 1.563 |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 445.100, 445.100, 445.100 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 2.900 |
| Data reduction software | PURDUE (DATA PROCESSING PACKAGE) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 3.000 |
| Rmerge | 0.124 |
| Total number of observations | 35325 * |
| Number of reflections | 33721 |
| Completeness [%] | 7.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | virus | 5 (mg/ml) | |
| 2 | 1 | drop | PEG8000 | 0.125 (%(w/v)) | or 0.25 %(w/v) |
| 3 | 1 | drop | Tris-HCl | 0.01 (M) | |
| 4 | 1 | reservoir | PEG8000 | 0.25 (%(w/v)) | or 0.5%(w/v) |
| 5 | 1 | reservoir | 0.02 (M) | ||
| 6 | 1 | reservoir | Tris-HCl | 0.01 (M) |
