1RTG

C-TERMINAL DOMAIN (HAEMOPEXIN-LIKE DOMAIN) OF HUMAN MATRIX METALLOPROTEINASE-2

Experimental procedure

Detector technology	IMAGE PLATE
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	55.780, 58.850, 93.140
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.600
R-factor	0.179
Rwork	0.179
RMSD bond length	0.011
RMSD bond angle	1.700
Data reduction software	MOSFLM
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	2.600 *	2.600 *
Rmerge	0.069	0.274 *
Total number of observations	34708 *
Number of reflections	9618
Completeness [%]	96.7	71.3 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6 *	20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	citrate	0.15 (M)
2	1	drop	PEG6000	2.5 (%)
3	1	reservoir	citrate	0.9 (M)