1RSN
RIBONUCLEASE (RNASE SA) (E.C.3.1.4.8) COMPLEXED WITH EXO-2',3'-CYCLOPHOSPHOROTHIOATE
Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | X11 |
Detector technology | IMAGE PLATE |
Collection date | 1992-11 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.700, 78.800, 39.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.119 |
RMSD bond length | 0.021 |
RMSD bond angle | 0.047 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.034 |
Total number of observations | 48382 * |
Number of reflections | 13932 * |
Completeness [%] | 98.4 * |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 3 (%) | |
2 | 1 | drop | sodium phosphate | 0.1 (M) | |
3 | 1 | reservoir | ammonium sulfate |