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1RRP

STRUCTURE OF THE RAN-GPPNHP-RANBD1 COMPLEX

Experimental procedure
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE BW7B
Synchrotron siteEMBL/DESY, HAMBURG
BeamlineBW7B
Temperature [K]100
Detector technologyAREA DETECTOR
Collection date1998-04
DetectorSIEMENS
Spacegroup nameC 1 2 1
Unit cell lengths121.339, 139.463, 91.654
Unit cell angles90.00, 135.78, 90.00
Refinement procedure
Resolution12.500 - 2.960
R-factor0.252
Rwork0.252
R-free0.30400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)RAN-GDP
RMSD bond length0.008
RMSD bond angle24.300

*

Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareCNS (0.4)
Refinement softwareCNS (0.4)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0003.000
High resolution limit [Å]2.9002.900
Rmerge0.0910.191
Total number of observations90705

*

Number of reflections20286
<I/σ(I)>13.13.1
Completeness [%]86.066
Redundancy4.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

6.25pH 6.25
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111PEG400018 (%)
211ammonium sulfate250 (mM)
311MES100 (mM)

227111

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