1RP3
Cocrystal structure of the flagellar sigma/anti-sigma complex, Sigma-28/FlgM
Experimental procedure
Experimental method | MAD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.388, 119.666, 100.056 |
Unit cell angles | 90.00, 107.00, 90.00 |
Refinement procedure
Resolution | 29.920 - 2.300 |
R-factor | 0.242 |
Rwork | 0.242 |
R-free | 0.26200 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.100 |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 76085 | |
<I/σ(I)> | 16 | 2.7 |
Completeness [%] | 99.9 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 16.2% PEG 8000, 0.09M SODIUM CACODYLATE, 0.18M CALCIUM ACETATE, 3% ISOPROPANOL, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K, pH 6.50 |