1RH7
Crystal Structure of Resistin-like beta
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2002-06-14 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.06975 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 57.604, 86.016, 283.406 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.960 - 3.106 |
R-factor | 0.20431 |
Rwork | 0.201 |
R-free | 0.26380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rgx |
RMSD bond length | 0.011 |
RMSD bond angle | 1.557 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 3.210 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.145 | 0.325 |
Number of reflections | 13231 | |
<I/σ(I)> | 20 | 9.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 2.5M NaCl, 0.1M Bis-Tris pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |