1RFY
Crystal Structure of Quorum-Sensing Antiactivator TraM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F2 |
Synchrotron site | CHESS |
Beamline | F2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-01-17 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9636 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 78.230, 85.750, 67.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.000 - 1.600 |
R-factor | 0.2021 |
Rwork | 0.202 |
R-free | 0.22200 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 1.000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SnB |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.061 | 0.403 |
Number of reflections | 29690 | |
<I/σ(I)> | 37.4 | 4.1 |
Completeness [%] | 98.5 | 84.8 |
Redundancy | 9.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | amonium acetate, sodium citrate, PEG 2000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |