1RE2
HUMAN LYSOZYME LABELLED WITH TWO 2',3'-EPOXYPROPYL BETA-GLYCOSIDE OF N-ACETYLLACTOSAMINE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1997-05 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.450, 62.300, 32.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
R-factor | 0.171 * |
Rwork | 0.171 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1REZ WITH SOLVENT MOLECULESOMITTED |
RMSD bond length | 0.011 |
RMSD bond angle | 24.900 * |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 62.300 |
High resolution limit [Å] | 2.250 |
Rmerge | 0.111 |
Total number of observations | 23021 * |
Number of reflections | 5742 |
<I/σ(I)> | 3.7 |
Completeness [%] | 96.8 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.5 | pH 4.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium nitrate | 3 (M) | |
2 | 1 | 1 | sodium acetate | 25 (mM) | |
3 | 1 | 1 | protein | 20 (mg/ml) | |
4 | 1 | 2 | ammonium nitrate | 5 (M) |