1RCU
X-RAY STRUCTURE OF TM1055 NORTHEAST STRUCTURAL GENOMICS CONSORTIUM TARGET VT76
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-09-14 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97879, 0.97907, 0.98027 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.748, 90.438, 83.210 |
Unit cell angles | 90.00, 94.56, 90.00 |
Refinement procedure
Resolution | 19.970 - 2.500 |
R-factor | 0.216 |
Rwork | 0.216 |
R-free | 0.23600 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.096 |
Number of reflections | 43759 |
Completeness [%] | 97.4 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 0.2M sodium Formate, 0.05M Tris, 18% PEG 3350, VAPOR DIFFUSION, HANGING DROP |