1RBP

CRYSTALLOGRAPHIC REFINEMENT OF HUMAN SERUM RETINOL BINDING PROTEIN AT 2 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	45.700, 48.700, 76.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.000
R-factor	0.181 *
Rwork	0.181
RMSD bond length	0.014
RMSD bond angle	3.100
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.090 *
Total number of observations	11088 *
Completeness [%]	85.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
2	1	reservoir	PEG6000
3	1	reservoir		0.5-1.2 (M)
4	1	reservoir	tris-(hydroxymethyl)aminomethane
5	1	reservoir		75 (mM)