1RAR

CRYSTAL STRUCTURE OF A FLUORESCENT DERIVATIVE OF RNASE A

Experimental procedure

Spacegroup name	P 32 2 1
Unit cell lengths	65.000, 65.000, 65.000
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.000 - 1.900
R-factor	0.172
RMSD bond length	0.012
RMSD bond angle	0.037 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.055 *
Total number of observations	33373 *
Number of reflections	11273 *
Completeness [%]	88.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5.1 *	20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop		3 (M)
2	1	drop	ammonium acetate	20 (%)
3	1	reservoir	acetate	50 (mM)