1RAL
THREE-DIMENSIONAL STRUCTURE OF RAT LIVER 3ALPHA-HYDROXYSTEROID(SLASH)DIHYDRODIOL DEHYDROGENASE: A MEMBER OF THE ALDO-KETO REDUCTASE SUPERFAMILY
Experimental procedure
Spacegroup name | C 2 2 21 |
Unit cell lengths | 51.300, 89.500, 143.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 3.000 |
R-factor | 0.22 |
Rwork | 0.220 |
RMSD bond length | 0.019 |
RMSD bond angle | 3.800 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 * |
High resolution limit [Å] | 3.000 * |
Rmerge | 0.098 * |
Total number of observations | 30872 * |
Number of reflections | 6122 * |
Completeness [%] | 96.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 5.8 * | 22 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG6000 | 25 (%(w/v)) | |
2 | 1 | reservoir | sodium citrate | 100 (mM) | |
3 | 1 | reservoir | ammonium sulfate | 120 (mM) |