1R9H

Structural Genomics of C.elegans: FKBP-type Peptidylprolyl Isomerase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2002-08-01
Detector	MAR CCD 165 mm
Wavelength(s)	1.0
Spacegroup name	P 61 2 2
Unit cell lengths	52.417, 52.417, 210.800
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.000 - 1.800
R-factor	0.21
Rwork	0.210
R-free	0.22700
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.300
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	38.130
High resolution limit [Å]	1.600
Number of reflections	21526

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	1.6M ammonium sulfate, 0.1M MES, 10% dioxane, seeding was used to grow the crystals, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K