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1R6J

Ultrahigh resolution Crystal Structure of syntenin PDZ2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X8C
Synchrotron siteNSLS
BeamlineX8C
Temperature [K]100
Detector technologyCCD
Collection date2003-04-11
DetectorADSC QUANTUM 4
Wavelength(s)0.85
Spacegroup nameP 1 21 1
Unit cell lengths25.876, 39.544, 32.276
Unit cell angles90.00, 109.64, 90.00
Refinement procedure
Resolution10.000 - 0.730
Rwork0.075
R-free0.08660
Structure solution methodAB INITIO
RMSD bond length0.019
RMSD bond angle0.033
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareSHELX
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0000.760
High resolution limit [Å]0.7300.730
Rmerge0.0600.387
Number of reflections71347
Completeness [%]83.99.6
Redundancy4.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7295PEG 4000, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K

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