1R6J
Ultrahigh resolution Crystal Structure of syntenin PDZ2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-04-11 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.85 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 25.876, 39.544, 32.276 |
Unit cell angles | 90.00, 109.64, 90.00 |
Refinement procedure
Resolution | 10.000 - 0.730 |
Rwork | 0.075 |
R-free | 0.08660 |
Structure solution method | AB INITIO |
RMSD bond length | 0.019 |
RMSD bond angle | 0.033 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 0.760 |
High resolution limit [Å] | 0.730 | 0.730 |
Rmerge | 0.060 | 0.387 |
Number of reflections | 71347 | |
Completeness [%] | 83.9 | 9.6 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | PEG 4000, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |