1R59
Enterococcus casseliflavus glycerol kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9788, 0.9791, 0.954, 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.829, 107.110, 201.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.500 |
Rwork | 0.221 |
R-free | 0.24300 |
Structure solution method | MIR |
RMSD bond length | 0.007 |
RMSD bond angle | 2.200 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.610 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.072 | 0.270 |
Number of reflections | 40746 | |
<I/σ(I)> | 9.7 | 5.4 |
Completeness [%] | 95.3 | 74.7 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.9 | 293 | PEG400, potassium phosphate, 1,10-phenanthroline, pH 5.9, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.9 | 293 | PEG400, potassium phosphate, 1,10-phenanthroline, pH 5.9, VAPOR DIFFUSION, HANGING DROP, temperature 293K |