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1R34

Golgi alpha-mannosidase II complex with 5-thio-D-mannopyranosylamidinium salt

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2002-09-11
DetectorMARRESEARCH
Spacegroup nameP 21 21 21
Unit cell lengths68.774, 109.568, 138.737
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.250 - 1.950
R-factor0.151
Rwork0.151
R-free0.19600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1hty
RMSD bond length0.020
RMSD bond angle1.900
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.020
High resolution limit [Å]1.9501.950
Rmerge0.1010.378
Number of reflections73805
<I/σ(I)>12.23.14
Completeness [%]94.895
Redundancy4.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7295PEG 6000, Tris, MPD, NaCl, pH 7.00, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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