1R2P

Solution structure of domain 5 from the ai5(gamma) group II intron

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE		600
2	Bruker	DMX		500
3	Bruker	DMX		750

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D NOESY
2	3	2	2D NOESY
3	4	2	2D NOESY
4	2	4	3D_13C-separated_NOESY
5	2	4	2D 1H-13C HSQC
6	2	2	2D 1H-1H TOCSY
7	2	4	3D 1H-13C-1H HCCH TOCSY
8	2	4	3D 1H-13C-1H HCCH COSY
9	2	3	2D 2JHN HNN-COSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5		278
2	6.5		298
3	6.5		308
4	6.5		291
5	6.5		303

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	10