1R1Y
Crystal structure of deoxy-human hemoglobin Bassett at 1.8 angstrom
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-09-27 |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.471, 82.246, 53.561 |
Unit cell angles | 90.00, 100.21, 90.00 |
Refinement procedure
Resolution | 49.240 - 1.800 |
R-factor | 0.183 |
Rwork | 0.183 |
R-free | 0.23600 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1g9v |
RMSD bond length | 0.013 |
RMSD bond angle | 19.100 * |
Data reduction software | bioteX |
Data scaling software | bioteX |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 82.250 | 1.850 |
High resolution limit [Å] | 1.850 | 1.800 |
Rmerge | 0.073 | 0.366 |
Number of reflections | 47432 | |
<I/σ(I)> | 33.7 | 1.57 |
Completeness [%] | 93.9 | 77.5 |
Redundancy | 2.9 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 | 298 | Perutz, M.F., (1968) J. Crystal Growth, 2, 54. * |