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1R12

Native Aplysia ADP ribosyl cyclase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE A1
Synchrotron siteCHESS
BeamlineA1
Temperature [K]200
Detector technologyCCD
Collection date1998-12-24
DetectorADSC QUANTUM 4
Wavelength(s)0.93
Spacegroup nameP 1 21 1
Unit cell lengths69.856, 58.503, 71.603
Unit cell angles90.00, 100.80, 90.00
Refinement procedure
Resolution25.000 - 1.700
R-factor0.209
Rwork0.208
R-free0.23790

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Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.018
RMSD bond angle1.865
Data reduction softwareDENZO
Data scaling softwareSCALA
Phasing softwareAMoRE
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.000
High resolution limit [Å]1.7001.700

*

Rmerge0.054

*

0.280

*

Number of reflections61981
Completeness [%]99.199.1

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Redundancy3.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

*

7.518

*

0.1 M Imidazole and 12-24 % PEG 4K, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 316K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirimidazole0.1 (M)pH7.5
21reservoirPEG400012-24 (%)

217705

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