1QZL
GCATGCT + Cobalt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-08-19 |
Detector | MARRESEARCH |
Wavelength(s) | 0.8416 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 24.789, 24.789, 91.818 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.570 - 2.850 |
R-factor | 0.24375 |
Rwork | 0.240 |
R-free | 0.33473 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.021 |
RMSD bond angle | 2.909 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.606 | 3.000 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.157 | 0.288 |
Number of reflections | 522 | |
<I/σ(I)> | 4.1 | 2.1 |
Completeness [%] | 96.7 | 99.5 |
Redundancy | 6.6 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 290 | sodium cacodylate, Cobalt dichloride, potassium chloride, MPD, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 290K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | sodium cacodylate | ||
2 | 1 | 1 | Cobalt dichloride | ||
3 | 1 | 1 | potassium chloride | ||
4 | 1 | 1 | MPD | ||
5 | 1 | 1 | H2O | ||
6 | 1 | 2 | sodium cacodylate | ||
7 | 1 | 2 | Cobalt dichloride | ||
8 | 1 | 2 | MPD | ||
9 | 1 | 2 | H2O |