1QWX

Crystal Structure of a Staphylococcal Inhibitor/Chaperone

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X25
Synchrotron site	NSLS
Beamline	X25
Temperature [K]	113
Detector technology	CCD
Collection date	2003-03-12
Detector	ADSC QUANTUM 4
Wavelength(s)	0.99876
Spacegroup name	P 21 21 21
Unit cell lengths	34.440, 77.910, 101.990
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	62.020 - 1.500
R-factor	0.2015
Rwork	0.200
R-free	0.22118
Structure solution method	SAD
RMSD bond length	0.018
RMSD bond angle	1.423
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	60.000
High resolution limit [Å]	1.500
Rmerge	0.050
Number of reflections	42519
Redundancy	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP			VAPOR DIFFUSION, HANGING DROP