1QWD
CRYSTAL STRUCTURE OF A BACTERIAL LIPOCALIN, THE BLC GENE PRODUCT FROM E. COLI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-06-15 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9393 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.999, 80.779, 88.953 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.140 - 1.750 |
R-factor | 0.17069 |
Rwork | 0.169 |
R-free | 0.20432 |
Structure solution method | SAD |
RMSD bond length | 0.020 |
RMSD bond angle | 1.696 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXD |
Refinement software | REFMAC (5.1.19) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.140 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.097 | 0.569 |
Number of reflections | 41968 | |
<I/σ(I)> | 14.5 | 1.8 |
Completeness [%] | 98.1 | 92.8 |
Redundancy | 5.4 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | NA-CITRATE, NA-BORATE, pH 7.50, VAPOR DIFFUSION, HANGING DROP, temperature 293K |