1QV4
B-DNA Dodecamer CGTGAATTCACG complexed with minor groove binder methylproamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 1997-10-11 |
Detector | SIEMENS |
Wavelength(s) | 0.71073 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 25.440, 40.640, 66.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.500 |
R-factor | 0.22 |
Rwork | 0.228 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 1.800 |
RMSD bond angle | 3.350 |
Data reduction software | SAINT (& SADABS) |
Data scaling software | SAINT |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 500.000 |
High resolution limit [Å] | 2.500 |
Number of reflections | 2513 |
Completeness [%] | 96.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |