1QTH
THE INTRODUCTION OF STRAIN AND ITS EFFECTS ON THE STRUCTURE AND STABILITY OF T4 LYSOZYME
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1997-10-29 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 31 |
Unit cell lengths | 53.569, 53.569, 101.871 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
Rwork | 0.189 |
RMSD bond length | 0.017 |
RMSD bond angle | 20.526 * |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.400 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.048 | 0.459 |
Number of reflections | 23171 | |
Completeness [%] | 85.0 * | 86.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.4 | 277 | PEG3.4K, magnesium chloride, Hepes, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | magnesium chloride | 20 (mM) | |
2 | 1 | 1 | HEPES | 0.1 (M) | |
3 | 1 | 1 | PEG3400 | 30 (%(w/v)) | |
4 | 1 | 1 | oxidized beta-mercaptoethanol |